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Innovative Curing of High Reliability Advnced Polymeric Encapsulants

机译:高可靠性高级聚合物密封剂的创新固化

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The presetn study evaluates a new curing method, the varibble Frequency Microwave technique, for processing high reliability adhesive encapsulants. THis process was used to cure three different high quality underfills wiht resultant properties that include low stress, no filler sedimentation , high glass transition temperature and good adhesion. For comparison, the same adhesives were also cured in a convection oven. Three different cure profiles were utilized to investigate their effects on the adhesive properties. These properties were analyzed with the following techniques: T sup g measurements were determined using Differential Scannign Calorimetry, adhesion measurements were derived through a standardized push-off test, stress was evaluated thrugh radiusof curvature measurements, and adhesive sedimentation was studied with Energy Dispersive spectroscopy. Infrared imaging was also used to evaluate the selective heating of the VFM cure. The results suggest that the VFM process is more rapid as ocmpared to the convection cure, i.e, 3.5 to 5 minutes as opposed ot 30 to 120 minutes. Furthermore, the VFM process resulted in a lower stress cure with equivalent mechanical properties of the polymer encapsulants.
机译:Presetn研究评估了一种新的固化方法,即可变频率微波技术,用于处理高可靠性的胶粘剂。该工艺用于固化三种不同的优质底部填充胶,其最终性能包括低应力,无填充剂沉降,高玻璃化转变温度和良好的附着力。为了比较,同样的粘合剂也在对流烘箱中固化。利用三种不同的固化曲线来研究它们对粘合性能的影响。使用以下技术分析这些性质:使用差示扫描量热法测定T的测量值,通过标准的推压试验得出粘附力的测量值,通过曲率半径测量评估应力,并使用能量分散光谱研究粘着剂的沉降。红外成像还用于评估VFM固化的选择性加热。结果表明,与对流固化相比,VFM过程更快,即3.5至5分钟,而对流固化则为30至120分钟。此外,VFM工艺可实现较低的应力固化,并具有与聚合物密封剂同等的机械性能。

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