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STABLE ELECTRON EMISSION FROM GRAPHITE-NANONEEDLES AND THEIR APPLICATION TO SCANNING ELECTRON MICROSCOPES

机译:石墨纳尼亚稳定的电子发射及其在扫描电子显微镜下的应用

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Nanometer sized carbon cathodes have attracted special interest from the point of view of high brightness electron sources. Recently achieved high brightness point electron emission from carbon nanotubes (CNTs) [1] and graphite-nanocrater (GRANC) [2] show promising aspects to downsize old-fashioned thermal emission devices such as micro-focus X-ray generators and electron microscopes. However, the drawbacks of these field emission (FE) sources for practical use are requirement of massive vacuum systems to obtain extremely low residual pressure less than 10{sup}(-9) torr. When these cathodes are operated at high residual pressure (10{sup}(-6) torr), these emission sources have problems related to current stability and longevity. Here we demonstrate both the stable and high brightness field emission from graphite nanoneedle (GRANN) cathode fabricated by simple plasma etching of a graphite rod [3]. Bright electron emission of the order of 10{sup}12 Asr{sup}(-1)m{sup}(-2) is obtained from GRANN cathode [4]. As well as the bright emission, a stable emission under high residual pressure (10{sup}(-5) torr) is obtained by lightly heating the GRANN cathode (Thermal-FE operation). The performance of the GRANN cathode is demonstrated by the construction of an FE scanning electron microscope (SEM) with the GRANN cathode and clear FE-SEM images are obtained at high residual pressure of the order of 10{sup}(-5) torr.
机译:纳米尺寸的碳阴极从高亮度电子来源的角度吸引了特别的兴趣。最近实现了来自碳纳米管(CNT)[1]和石墨 - 纳克拉特(Granc)[2]的高亮度点电子发射,表明了对诸如微聚焦X射线发生器和电子显微镜等老式的热发射装置进行缩小的有希望的方面。然而,用于实际使用的这些场发射(Fe)源的缺点是大规模真空系统的要求,以获得极低的残余压力小于10 {sup}( - 9)托。当这些阴极以高剩余压力(10 {SUP}( - 6)Torr)操作时,这些发射源具有与当前稳定性和寿命相关的问题。在这里,我们通过简单的等离子体蚀刻石墨棒的简单等离子体蚀刻来证明稳定和高亮度场发射[3]。从Grann阴极[4]获得10 {sup} 12asr {sup}( - sup}( - 1)m {sup}(-2)的亮度的电子发射。除了明亮的发射,通过轻轻加热GRANN阴极(Thermal-Fe操作),获得高残余压力(10 {sup}( - 5)托的稳定发射。通过用Grann阴极的扫描电子显微镜(SEM)构造来证明Grann阴极的性能,并且在10 {SUP}( - 5)托的高剩余压力下获得清晰的FE-SEM图像。

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