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Low pressure infiltration of molten aluminum alloy to C/C preform with nickel plating

机译:镀镍使熔融铝合金低压渗透到C / C预成型坯中

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As the wetability between carbon and aluminum alloy is very low, carbon / aluminum composites usually fabricate by the squeeze casting process. In this study, in order to fabricate the carbon fiber reinforced carbon (C/C) reinforced aluminum alloy matrix composites by low-pressure infiltration process (under 1MPa), nickel (Ni) plating on carbon fiber in C/C perform was examined. In order to obtain the thin and homogeneous Ni film on carbon fiber in preform, activator process with tin (Sn) containing bases solution and sensitizer process with palladium (Pd) containing bases solution was pre-treated before Ni plating. Furthermore, in order to obtain the homogeneous plating in all position in preform, Ni plating was examined with the assistance of ultrasonic vibration and one directional flow of plating solution using pump. One directional flow was suitable for the homogeneous plating. Then, the optimum conditions of Ni plating were obtained as 353 K and 120s for temperature and time, respectively. Finally, the preparation of C/C reinforced aluminum composites were examined by low pressure infiltration process. The infiltration behavior of molten aluminum alloy (AA332.0) was identified above 0.2 MPa in applied pressure. As increasing the infiltration pressure till 0.5 MPa, the infiltration ability of molten aluminum alloy increased.
机译:由于碳与铝合金之间的润湿性非常低,因此通常通过挤压铸造工艺来制造碳/铝复合材料。在这项研究中,为了通过低压渗透工艺(在1MPa以下)制造碳纤维增强的碳(C / C)增强铝合金基复合材料,研究了碳/碳在碳纤维上镀镍(Ni)的性能。为了在预制棒上在碳纤维上获得均匀的薄镍膜,在镀镍之前先对含锡(Sn)的碱溶液进行活化剂处理,并对含钯(Pd)的碱溶液进行敏化处理。此外,为了在预成型坯的所有位置获得均匀的镀层,借助于超声振动和使用泵的镀液的单向流动,对Ni镀层进行了检查。一种定向流适合于均匀镀覆。然后,获得的最佳镀镍条件为温度和时间分别为353 K和120s。最后,通过低压渗透法对C / C增强铝复合材料的制备进行了研究。在施加压力超过0.2 MPa时,确定了熔融铝合金(AA332.0)的渗透行为。随着渗透压力增加到0.5MPa,熔融铝合金的渗透能力增加。

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