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Study on the Microstructure and the Machining Performance of Ti_3SiC_2-TiB_2-TiC Composite Ceramic

机译:TI_3SIC_2-TIB_2-TIC复合陶瓷微观结构及加工性能研究

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The Ti_3SiC_2-TiB_2-TiC three-phase ceramics are prepared by Spark Plasma Sintering (SPS) method with Self-propagating High-temperature Synthesis (SHS) using Ti, Si, C andB_4C powders. The characterization of sintering product's image and structure is analyzed by XRD and SEM. Most of TiB_2's images are angular cuboid or short bar-shaped and most of TiC phase's images are irregular spherical particles which are evenly embedded in Ti_3SiC_2 substrate and have a good combination interface with Ti_3SiC_2. In the composite ceramic SPS sintering process, sinter sample's displacement along Z-axis goes through three stages of falling, balance and rising along with the change of heating temperature, which reflects the sample's change rule between heated expansion force and pressure. Finally its machining performance is analyzed by wire cutting method and machining method. The Ti_3SiC_2-TiC-TiB_2 block composite ceramic proves to have a good machining performance.
机译:通过使用Ti,Si,C andB_4C粉末通过Spark等离子体烧结(SPS)方法制备Ti_3SIC_2-TIB_2-TIC三相陶瓷。通过XRD和SEM分析烧结产品的图像和结构的表征。大多数TIB_2的图像是角型长方体或短条形,并且大多数TIC相位的图像是不规则的球形颗粒,其均匀地嵌入Ti_3SIC_2基板中,并且具有与Ti_3SIC_2的良好组合界面。在复合陶瓷SPS烧结过程中,烧结样品沿Z轴的位移通过三个阶段的下降,平衡和上升以及加热温度的变化,这反映了加热膨胀力和压力之间的样品的变化规则。最后通过钢丝切割方法和加工方法分析其加工性能。 Ti_3SIC_2-TIC-TIB_2块复合陶瓷证明具有良好的加工性能。

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