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A New Gravimetric – Swelling Test for Evaluating Water and Ion Uptake in Shales

机译:用于评估页岩中水分和离子吸收的新的重量分析法

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The primary cause of wellbore instability is the interaction of water-based muds with shales. The movement of water and ions into or out of a shale can result in large changes in pore pressure in the vicinity of the wellbore, potentially leading to wellbore failure. A new method, the Gravimetric – Swelling Test (GST), for determining the compatibility between shales and drilling fluids is presented in this paper. An experimental protocol and equations are presented that describe how such measurements can be conducted and interpreted with relative ease. The mass of water and ions entering or leaving shale samples is determined. With additional swelling measurements, the impact of the water and ions uptake on swelling pressures generated can also be obtained. In this paper, results are presented for two preserved shale samples obtained from the field. The influence of different types of ionic solutions on water and ion movement is presented for each shale. It is shown that water uptake and swelling of shales is controlled not only by differences between shale water activity and water activity in the mud (as assumed in the past), but ion type and concentration also play an important role. In these tests the water uptake decreases, while the ion adsorption increases with increasing salt concentration. Different types of cations are shown to have a large influence on water/ion movement. This paper presents a data set showing the influence of ion type and concentration on water uptake by shales. The role of capillary pressure, osmotic effects and ionic diffusion on swelling behavior of shales is also discussed. The technique presented herein may possibly be used at the rigfloor to determine the compatibility of shales with salt-water drilling fluids.
机译:井筒不稳定的主要原因是水基泥浆与页岩的相互作用。水和离子进入或离开页岩的运动可能会导致井眼附近的孔隙压力发生较大变化,从而可能导致井眼发生故障。 本文介绍了一种用于确定页岩和钻井液之间相容性的新方法,即重量膨胀试验(GST)。提供了一个实验协议和方程式,描述了如何相对轻松地进行和解释此类测量。确定进入和离开页岩样品的水和离子的质量。通过附加的溶胀测量,还可以获得水和离子吸收对产生的溶胀压力的影响。 本文介绍了从田间获得的两个保存完好的页岩样品的结果。每种页岩都提出了不同类型的离子溶液对水和离子运动的影响。结果表明,页岩的吸水和溶胀不仅受页岩水活度和泥浆中水活度之间差异的控制(如过去所假设的),而且离子类型和浓度也起着重要的作用。在这些测试中,吸水率降低,而离子吸附随着盐浓度的增加而增加。已显示不同类型的阳离子对水/离子运动有很大影响。 本文提供了一个数据集,显示了离子类型和浓度对页岩水吸收的影响。还讨论了毛细压力,渗透作用和离子扩散对页岩溶胀行为的作用。本文介绍的技术可能会在钻井平台上用于确定页岩与盐水钻井液的相容性。

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