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Application of Scannign probe Microscopy Nano-indentation towards Nanomechanical Characterization of Polymer Films

机译:扫描探针显微镜纳米压痕在聚合物膜纳米力学表征中的应用

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The extremely high measurement sensitivity and accuracy has made scanning probe microscopy a valuable tool for detecting various kinds of tip surface interactions such as Van der Waals force for AFM, electron tunneling for STM, electric magnetic forces for EFM/MFM, frictional force for LFM, etc. This paper presents a enw technique, SPM nano-indentation technique, for monitoring the repulsive forcebetween the sharp probe nad material surfaceas a means to detect the mechanical properties of materials. The key advantages of SPM nano-indentation are its imaging capability which allows accurate measurement of indentation teometry and precise location of indentation probe for nanomechanical measurement. This particular study explores the areas of applicability fo SPM for measuring mechanical propertics such as young's modulus of materials. Limit studies have been done in understandignthe reproducibility of force curves, the effectof surface roughness on force curve, substrate on Young's modulus measurement, etc. Examples of Young's modulus extraction for organic films will be presented.
机译:极高的测量灵敏度和准确性使扫描探针显微镜成为检测各种尖端表面相互作用的有价值的工具,例如用于AFM的范德华力,用于STM的电子隧穿,用于EFM / MFM的电磁力,用于LFM的摩擦力,本文提出了一种enw技术,即SPM纳米压痕技术,用于监测尖锐的探针和材料表面之间的排斥力,以此作为检测材料的机械性能的手段。 SPM纳米压痕的关键优势在于其成像功能,可以精确地测量压痕测距法和用于纳米机械测量的压痕探针的精确位置。这项特殊的研究探索了SPM在测量机械特性(例如材料的杨氏模量)方面的适用性领域。在理解力曲线的可再现性,表面粗糙度对力曲线的影响,基材对杨氏模量的测量等方面已经进行了极限研究。将给出有机膜的杨氏模量提取的实例。

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