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An Investigation of the Mechanical Properties And Fracture Characteristic of Hot-Pressed Boron Nitride Ceramics

机译:热压氮化硼陶瓷的力学性能和断裂特性研究

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The overall mechanical characterization of hot-pressed hexagonal boron nitride (h-BN) based ceramics was performed. Hardness, flexure strength and fracture toughness (K_(IC)) measurements were carried out using Vickers indentations, 3-point bending tests and SEVNB method, respectively. The fracture characteristics of hot-pressed h-BN ceramics were investigated by analyzing fracture surfaces using scanning electron microscope (SEM). The hardness, ranged from Hv = 0.20GPa to Hv = 0.25GPa, which was higher in the surfaces parallel to the hot-press direction due to the perpendicular alignment of the basal planes of the h-BN platelets to the hot-press direction. The fracture toughness and flexure strength values were determined to be 2.6 MPa.m~(1/2) and 0.14 GPa, respectively. A single K_(IC) value was obtained since a slight variation of the fracture toughness was observed with the orientation of h-BN, The microstructural observations of h-BN grains indicated completely brittle fracture with intergranular voids and microcracks revealing a mixed mode of fracture.
机译:进行了热压六角形氮化硼(h-BN)基陶瓷的整体机械性能表征。分别使用维氏压痕,三点弯曲试验和SEVNB方法进行硬度,弯曲强度和断裂韧性(K_(IC))测量。通过使用扫描电子显微镜(SEM)分析断裂表面,研究了热压h-BN陶瓷的断裂特性。硬度在Hv = 0.20GPa到Hv = 0.25GPa的范围内,这是由于h-BN血小板的基面垂直于热压方向而在平行于热压方向的表面上较高。断裂韧性和弯曲强度值分别确定为2.6 MPa.m〜(1/2)和0.14 GPa。由于观察到h-BN取向时断裂韧性略有变化,因此获得了一个单一的K_(IC)值。h-BN晶粒的显微组织观察表明,完全脆性断裂是晶间空隙和微裂纹,表明混合断裂模式。

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