A Study for Synthesis of Nanobelt and Nanowire Nickel Powders by Wet Chemical Method

摘要

Ni nanosheet has been prepared at various temperature and time with anion surfactant by chemical reduction of the nickel ion complexes formed from complexing reagent in a pressurized vessel. Sample was characterized by the means of an X-ray diffractomer (XRD), a field emission scanning electron microscopy (FESEM), an energy dispersive X-ray spectrometer (EDS), a selected-area electron diffraction (SAED) and a high sensitive magnetometer (HSM). The use of SDBS and sodium tartrate could be a key factor for the formation and growth of Ni nanosheet.