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Preparation and Characterization Upconversion Luminescence Material of Yttrium Aluminate Doped with Rare Earth

机译:稀土掺杂铝酸钇的上转换发光材料的制备与表征

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Low phonon energy yttrium aluminate was adopted as matrix and the upconversion materials yttrium aluminate co-doped with Yb3 + and Er3 + was synthesized by solid-state reaction method. The X-ray diffraction spectra and the upconversion emission spectra of various samples were measured and the effect of Er3+ concentration , sensitization, fluxing agent and calcining temperature on the luminescence properties was studied. Research results showed that the sample could emit green light at 543 and 570 nm when excited 980 nm laser; the optimum concentration of Er3+ should be 1.0%; sensitization of Yb3+ could enhance luminescent effects of Er3 + obviously; the optimum content of H3BO3 fluxing agent should be 8% and the optimum calcining temperature should be 1500 ℃.
机译:以低声子能铝酸钇为基体,通过固相反应法合成了Yb3 +和Er3 +共掺杂的上转换材料铝酸钇。测量了各种样品的X射线衍射光谱和上转换发射光谱,并研究了Er3 +浓度,敏化度,助熔剂和煅烧温度对发光性能的影响。研究结果表明,当激发980 nm激光时,样品可以发射543和570 nm的绿光。 Er3 +的最佳浓度应为1.0%; Yb3 +的敏化作用可以明显增强Er3 +的发光效果。 H3BO3助熔剂的最佳含量应为8%,最佳煅烧温度应为1500℃。

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