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Influence of Binder Additives on the Sintering of Nano-3Y-TZP

机译:粘结剂对纳米3Y-TZP烧结的影响

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摘要

Nanosized yttria stabilized tetragonal zirconia powders were prepared by chemical co-precipitation. By adding certain amount of wax emulsion, we obtained green compacts with the relative density ranged from 47% to 60%. Then the green compacts were sintered in air at the temperature from 1350℃ to 1550℃. It turned out that the 3Y-TZP compacts were nearly fully densified after sintering at 1350℃ and the grain sizes were between 200 to 300 nm. This result suggested that the addition of wax emulsion could improve the wettability between powders, elevated the density of the green compacts so that the coordination number and the contact points between particles were increased. With more transfer passages, the sintering behavior is remarkably improved.
机译:通过化学共沉淀制备纳米级的氧化钇稳定的四方氧化锆粉末。通过添加一定量的蜡乳液,我们获得了相对密度为47%至60%的生压坯。然后将生坯在空气中在1350℃至1550℃的温度下烧结。结果表明,在1350℃下烧结后3Y-TZP压坯几乎完全致密化,晶粒尺寸在200至300 nm之间。该结果表明,添加蜡乳液可以改善粉末之间的润湿性,提高生坯的密度,从而增加了配位数和颗粒之间的接触点。随着传递通道的增加,烧结性能得到显着改善。

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