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Solution Heat Treatment of Single Crystal Superalloy with Electric Field

机译:单晶高温合金的固溶热处理

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The effect of a DC electric field on solution heat treatment of Ni-based single crystal superalloy DD3 was investigated by means of optical metallograph, scanning electron micrograph (SEM) and electron probe microanalysis (EPMA). The superalloy samples were heat-treated at 1220, 1230, 1240 and 1250"C for four hours under the electric field E= 1000 V/cm, respectively. The experimental results showed that: a) the electric field solution heat treatment (EFSHT) enhanced microstructure homogenization; b) the distributions of alloy elements, especially the refractory metal elements Mo and W, were more homogeneous after EFSHT; and c) EFSHT enhanced dissolution and reduced-solvus temperature. The likely mechanism was that the electric field enhanced the migration of the vacancies from the interior to the surface, which increased the diffusion rate of atoms.
机译:通过光学金相,扫描电子显微镜(SEM)和电子探针显微分析(EPMA)研究了直流电场对Ni基单晶高温合金DD3固溶热处理的影响。高温合金样品分别在电场E = 1000 V / cm下于1220、1230、1240和1250“ C热处理4小时。实验结果表明:a)电场溶液热处理(EFSHT) EFSHT后,合金元素,特别是难熔金属元素Mo和W的分布更加均匀; c)EFSHT增强了溶解,降低了固溶温度;可能的机理是电场增强了迁移从内部到表面的空位,增加了原子的扩散速率。

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