A Convenient Procedure for the Preparation of Levoglucosenone and Its Conversion to Novel Chiral Derivatives

机译：左旋葡糖酮的制备及其向新型手性衍生物的转化的简便方法

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As part of a study to develop methods to obtain high-value nonracemic chiral compounds from biomass, we have developed a convenient method for converting cellulose to levoglucosenone in > 10% yield. This procedure and methods to convert levoglucosenone into potentially useful chiral derivatives are presented.

机译：作为开发从生物质中获得高价值非外消旋手性化合物的方法的研究的一部分，我们已经开发了一种方便的方法，可将纤维素转化为左旋葡糖醛酮，产率> 10％。提出了将左葡糖苷酮转化为潜在有用的手性衍生物的方法和方法。

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来源
《American Chemical Society(ACS) National Meeting; 20000326-20000330; San Francisco,CA; US》|2000年|P.21-31|共11页
会议地点 San Franciso CA(US);San Franciso CA(US)
作者
Walter S. Trahanovsky; Jason M. Ochaoda; Chen Wang; Kevin D. Revell; Kirk B. Arvidson; Yu Wang; Huiyan Zhao; Steven Chung; Synthia Chang;
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Department of Chemistry, Iowa State University, Ames, IO 50011-3111;

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正文语种 eng
中图分类化学纤维工业;
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专利

1. A CONVENIENT PROCEDURE FOR THE REDUCTION OF S-(+)-SILYL SERINE METHYL ESTER TO CHIRAL SERINOL DERIVATIVES [J] . Novachek KA., Meyers AI. Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 1996,第11期

机译：S-（+）-甲硅烷基丝氨酸甲酯还原为手性三联醇衍生物的简便方法
2. Reductive ring opening of 6-deoxy-6-iodopyranosides and 5-deoxy-5-iodofuranosides by manganese. A convenient procedure for the preparation of chiral 5-hexenals and 4-pentenals [J] . Tanaka K., Mitsunobu O., Yamano S. Synlett . 2001,第10期

机译：锰对6-脱氧-6-碘吡喃糖苷和5-脱氧-5-碘呋喃糖苷的还原性开环。制备手性5-己烯醛和4-戊烯醛的简便方法
3. A CONVENIENT PROCEDURE FOR THE CONVERSION OF N-BOC PROTECTED PYRROLIDINONE DERIVATIVES INTO THEIR CORRESPONDING ENECARBAMATES [J] . Cossy J., Pardo DG., Cases M. Synthetic Communications . 1997,第16期

机译：将N-BOC保护的吡咯烷酮衍生物转化为相应的氨基甲酸酯的简便方法
4. A Convenient Procedure for the Preparation of Levoglucosenone and Its Conversion to Novel Chiral Derivatives [C] . Walter S. Trahanovsky, Jason M. Ochaoda, Chen Wang, American Chemical Society . 2003

机译：制备左葡葡萄酒的方便步骤及其对新型手性衍生物的转化
5. Formation of gamma-lactams and lactones by radical cyclizations, homolytic aromatic alkylations, and preparation of levoglucosenone and its chiral derivatives. [D] . Wang, Chen. 1999

机译：通过自由基环化，均相芳族烷基化以及制备左旋葡萄糖醛酮及其手性衍生物来形成γ-内酰胺和内酯。
6. Efficient oxidation of oleanolic acid derivatives using magnesium bis(monoperoxyphthalate) hexahydrate (MMPP): A convenient 2-step procedure towards 12-oxo-28-carboxylic acid derivatives [O] . Jorge A R Salvador, Vânia M Moreira, Rui M A Pinto, 2012

机译：使用双（邻过氧邻苯二甲酸酯）六水合镁（MMPP）高效氧化齐墩果酸衍生物：方便的两步法制备12-氧代-28-羧酸衍生物
7. Formation of [gamma]-lactams and lactones by radical cyclizations, homolytic aromatic alkylations, and preparation of levoglucosenone and its chiral derivatives [O] . Wang, Chen 1999

机译：通过自由基环化，均相芳族烷基化以及左旋葡糖酮及其手性衍生物的制备形成γ-内酰胺和内酯
8. Chiral Synthesis via Organoboranes. 33. The Controlled Reaction of B-Alkydiisopinocampheylboranes with Aldehydes Providing a Convenient Procedure for the Enantiomeric Enrichment of the Boronic Ester Products Through Kinetic Resolution [R] . Joshi, N. N., Pyun, C., Mahindroo, V. K., 1991

机译：有机硼烷的手性合成。 33.B-烷基异哌啶基硼烷与醛的可控反应通过动力学拆分提供了对硼酸酯产物对映体富集的方便程序

A Convenient Procedure for the Preparation of Levoglucosenone and Its Conversion to Novel Chiral Derivatives

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