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Method for Synthesizing Diaza-Bridged Compound and a Diaza-Bridged Compound
Method for Synthesizing Diaza-Bridged Compound and a Diaza-Bridged Compound
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机译:重氮桥联化合物的合成方法和重氮桥联化合物
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摘要
The present disclosure discloses a method for synthesizing a diaza-bridged compound and a diaza-bridged compound, belonging to the field of organic synthesis. The present disclosure includes the following reaction:; ;in the formula, R is aryl, substituted aryl, alkyl or haloalkyl, Ra is any one of H, 2-nitrobenzenesulfonyl, 4-nitrobenzenesulfonyl or 2,4-dinitrobenzenesulfonyl, n=1 or 2. Since compound 2 and NH3 are used as raw materials, the present disclosure can not only effectively shorten the process flow and save process costs, but also improve the reaction yield to a certain extent. The present disclosure also provides a diaza-bridged compound, where the structural formula thereof is; ;in the formula, Ra is any one of 2-nitrobenzenesulfonyl, 4-nitrobenzenesulfonyl or 2,4-dinitrobenzenesulfonyl. Since the compound has a higher melting point, is easy to recrystallize to get solid and not easy to form oil under high temperature, the diaza-bridged compound is suitable for long-distance transportation and long-term storage.
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