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METHOD FOR PREPARING CATIONIC POLYACRYLAMIDE FLOCCULANT

机译:制备阳离子聚丙烯酰胺絮凝剂的方法

摘要

Disclosed is a method for preparing a cationic polyacrylamide flocculant. The method has the following steps: adding a DAC aqueous solution with a mass fraction of 80%, AM and distilled water to a four-neck flask equipped with a stirrer and a thermometer, uniformly mixing same, introducing nitrogen to evacuate air from the system, heating same in a water bath to 54-58°C, adding a tert-butyl hydrogen peroxide initiator and sodium pyrosulfite, continuing to introduce nitrogen for 2-4 h, carrying out a polymerization reaction under closed conditions for 8-10 h, then removing a colloid, soaking same with acetone for 25-27 h, then soaking same with absolute ethanol for 25-27 h, drying a white solid in a vacuum drying oven at 50-60°C for 5-7 h, and drying and crushing same to obtain the flocculant. The method is simple, convenient, quick and easy to operate, and the prepared cationic polyacrylamide flocculant has a high removal rate in terms of wastewater turbidity and can be prepared on a large scale.
机译:公开了一种制备阳离子聚丙烯酰胺絮凝剂的方法。该方法具有以下步骤:将具有80%,AM和蒸馏水的质量分数的DAC水溶液加入配备有搅拌器和温度计的四颈瓶中,均匀混合,引入氮气从系统中抽空空气,在水浴中加热至54-58℃,加入叔丁基过氧化氢引发剂和吡咯硫酸钠,继续引入2-4小时,在闭合条件下进行聚合反应8-10小时,然后除去胶体,浸泡与丙酮相同25-27小时,然后浸泡与绝对乙醇相同25-27小时,在真空干燥烘箱中在50-60℃下干燥白色固体5-7小时,并干燥并压碎相同,以获得絮凝剂。该方法简单,方便,快速且易于操作,并且制备的阳离子聚丙烯酰胺絮凝剂在废水浊度方面具有高的去除率,并且可以大规模制备。

著录项

  • 公开/公告号WO2021237379A1

    专利类型

  • 公开/公告日2021-12-02

    原文格式PDF

  • 申请/专利号WO2020CN91947

  • 发明设计人 TAN LING;

    申请日2020-05-23

  • 分类号C08F220/34;C08F220/56;C02F1/56;

  • 国家 CN

  • 入库时间 2022-08-24 22:37:29

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