首页> 外国专利> Method for manufacturing epoxy compound for optical materials and method for manufacturing episulfide compound for optical material and high refractive optical material using same

Method for manufacturing epoxy compound for optical materials and method for manufacturing episulfide compound for optical material and high refractive optical material using same

机译:用于光学材料的环氧化合物的制造方法及用于制造光学材料外观化合物的方法和使用相同的高折射光学材料

摘要

The present invention relates to a method of manufacturing an epoxy compound for an optical material, and a method for manufacturing an episulfide compound for an optical material and a high refractive optical material using the same. In the present invention, epichlorohydrin and hydrogen sulfide are reacted to obtain bis(3-chloro-2-hydroxypropyl)sulfide, and the bis(3-chloro-2-hydroxypropyl)sulfide obtained in the above step is used as an alkali. A method for preparing an epoxy compound comprising the step of obtaining bis(2,3-epoxypropyl)sulfide represented by the following formula (1) by reacting with There is provided a method for producing an epoxy compound for an optical material, characterized in that the reaction is carried out while maintaining the initial reactor temperature at 15 to 40° C. using 12 to 50% by weight of caustic soda. According to the present invention, it is possible to manufacture a high-quality epoxy compound for an optical material with a low content of impurities and no yellowish color. can be manufactured.
机译:本发明涉及一种制造用于光学材料的环氧化合物的方法,以及用于制造用于光学材料的外观化合物的方法和使用该方法的高折射光学材料。在本发明中,反应上氯醇和硫化氢以获得双(3-氯-2-羟丙基)硫化物,并使用上一步中得到的双(3-氯-2-羟丙基)硫化物作为碱。制备包含由下式(1)代表的双(2,3-环氧丙基)硫化物通过与其中反应提供的双(2,3-环氧丙基)硫化物的步骤的方法提供了一种用于光学材料的环氧化合物,其特征在于进行反应,同时使用12至50重量%的苛性钠将初始反应器温度保持在15至40℃。根据本发明,可以制造具有低含量的杂质和淡黄色的光学材料的高质量环氧化合物。可以制造。

著录项

  • 公开/公告号KR20210130547A

    专利类型

  • 公开/公告日2021-11-01

    原文格式PDF

  • 申请/专利权人 주식회사 엠엘텍;

    申请/专利号KR20200048914

  • 发明设计人 장동규;노수균;

    申请日2020-04-22

  • 分类号C07D303/34;C07D331/02;C07D409/12;C08G18/38;C08G75/06;G02B1/04;

  • 国家 KR

  • 入库时间 2022-08-24 22:26:52

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