Transition Metal Electrochemical Catalyst Using Synthetic Rapid Combustion and Synthesis Method thereof

摘要

The present invention relates to a transition metal electrochemical catalyst and a synthesis method thereof using an ultra rapid combustion method, and more specifically, a solution in which a transition metal ion and a free group anion are coordinated by dissociating a nitrogen precursor and a transition metal precursor in a polyol-based solvent. A) step of preparing a mixture by preparing and mixing it with a support; Step b) of igniting the mixture prepared in step a) to carbonize the polyol-based solvent to form transition metal nanoparticles surrounded by carbon; C) performing heat treatment to carbonize residual organic matter contained in the mixture; And removing the transition metal nanoparticles and impurities that are not surrounded by carbon through acid treatment, and then removing residual acid through washing and re-heat treatment; including, but through the steps a) to d). It is characterized by synthesizing a nanocatalyst having a monoatomic transition metal-nitrogen bond structure and a transition metal nanoparticle surrounded by carbon at the same time or in the presence of one of the two.