A lithiated carbon phosphonitride material is made by, for example, reacting P(CN)3 with LiN(CN)2 in solution (for example, dimethoxyethane or pyridine), then drying the solution to obtain the product. The material is a thermoset that is stable to over 400° C. and exhibits up to 10−3 S·cm2 of Li+ conductivity.
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