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Method for mass production of carbon nanotubes by alkali metal catalyst and carbon nanotube synthesized from it

机译:用碱金属催化剂和碳纳米管碳纳米管碳纳米管的大规模生产方法

摘要

The present invention relates to a method for mass synthesis of carbon nanotubes using an alkali metal catalyst and to carbon nanotubes synthesized therefrom, and more particularly, without using a non-alkali metal catalyst such as iron, cobalt, nickel, and excluding hydrogen. It relates to the synthesis of pure carbon nanotubes using an alkali metal catalyst based on a group 1 element. The present invention comprises the steps of preparing a carbon source; Dissolving an alkali metal-based alkali metal-containing compound in a solvent to form an alkali metal catalyst precursor solution; By heat treatment while spraying the alkali metal catalyst precursor solution while supplying the carbon source, the alkali metal of the sprayed alkali metal catalyst precursor solution is aggregated into the nano catalyst, and the carbon source is dissolved and crystallized in the nano catalyst to grow carbon nanotubes. The nanocatalyst is evaporated while being removed; a method for mass synthesis of carbon nanotubes using an alkali metal catalyst, characterized in that it includes, and carbon nanotubes synthesized therefrom, as a technical point.
机译:本发明涉及使用碱金属催化剂和由其合成的碳纳米管来大量合成碳纳米管的方法,更具体地,不使用诸如铁,钴,镍和排除氢的非碱金属催化剂。它涉及使用基于第1组元素的碱金属催化剂的纯碳纳米管的合成。本发明包括制备碳源的步骤;将碱金属基碱金属化合物溶解在溶剂中以形成碱金属催化剂前体溶液;通过热处理在供应碳源的同时喷涂碱金属催化剂前体溶液,喷涂的碱金属催化剂前体溶液的碱金属聚集到纳米催化剂中,并将碳源溶解并在纳米催化剂中结晶以生长碳纳米管。纳米催化剂在除去时蒸发;一种使用碱金属催化剂对碳纳米管进行大规模合成碳纳米管的方法,其特征在于它包括和由其合成的碳纳米管,作为技术点。

著录项

  • 公开/公告号KR20210029985A

    专利类型

  • 公开/公告日2021-03-17

    原文格式PDF

  • 申请/专利权人 한국해양대학교 산학협력단;

    申请/专利号KR1020190111345

  • 发明设计人 강준;김대영;

    申请日2019-09-09

  • 分类号C01B32/162;B01J31/02;

  • 国家 KR

  • 入库时间 2022-08-24 17:44:50

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