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Three-component simultaneous analyzer and three-component simultaneous analysis method

机译:三组分同时分析仪和三组分同时分析方法

摘要

This three-component simultaneous analysis device is a device for detecting three components, comprising methane gas, carbon dioxide and nitrous oxide, contained in atmospheric gas, which is an assay sample. The three-component simultaneous analysis device includes: a first gas flow passage (A); a second gas flow passage (B) and a third gas flow passage (C) located downstream of the first gas flow passage (A); and a switching valve (400) which is located between the first gas flow passage (A) and the second gas flow passage (B) and between the first gas flow passage (A) and the third gas flow passage (C), and which is used to switch between a first state in which the first gas flow passage (A) and the second gas flow passage (B) communicate with one another, and a second state in which the first gas flow passage (A) and the third gas flow passage (C) communicate with one another. The first gas flow passage (A) includes a first column (60) disposed in order to obtain a first gas phase including methane gas, and a second gas phase including carbon dioxide and nitrous oxide. The second gas flow passage (B) includes a hydrogen flame ionization detector (100). The third gas flow passage (C) includes: a second column (70) comprising a packed column; a third column (80) which is downstream of the second column (70), comprises a capillary column or a stainless steel column, and is disposed in order to obtain a third gas phase including carbon dioxide and a fourth gas phase including nitrous oxide; a thermal conductivity detector (200); and an electron capture detector (300).
机译:该三组分同时分析装置是用于检测包含在大气气体中的甲烷气体,二氧化碳和氧化氮的三种组分的装置,其是测定样品。三组分同时分析装置包括:第一气流通道(A);第二气体流动通道(B)和位于第一气流通道(A)下游的第三气体流动通道(C);和位于第一气体流动通道(A)和第二气流通道(B)之间以及第一气流通道(A)和第三气流通道(C)之间的切换阀(400),以及用于切换第一状态,其中第一气流通道(a)和第二气流通道(b)彼此连通,以及第一气流通道(a)和第三气体的第二状态流动通道(c)彼此沟通。第一气体流动通道(A)包括设置的第一柱(60),以便获得包括甲烷气体的第一气相和包括二氧化碳和氧化亚氮的第二气相。第二气体流动通道(B)包括氢火焰电离检测器(100)。第三气体流动通道(c)包括:第二柱(70),其包含填充柱;在第二柱(70)下游的第三柱(80)包括毛细管柱或不锈钢柱,并设置为获得包括二氧化碳的第三气相和包括一氮的第四气相;导热探测器(200);和电子捕获探测器(300)。

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