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Readily soluble basic colouring matters

机译:易溶的基本色素

摘要

Basic colouring matters are made readily soluble in water by admixture of the free base with sulphamic acid, or by mixing a salt of the free base with a salt of sulphamic acid and, if necessary, drying, or by conversion of the free base into a sulphamate by reacting it with sulphamic acid or by reacting a salt thereof with a soluble salt of sulphamic acid. In examples: (1) Rhodamine B base powder is mixed with powdered sulphamic acid; (2) Victoria blue B or R base is ground with sulphamic acid; (3) Acridine orange base powder is mixed with powdered sulphamic acid; (4) the free base of the condensation product from 4 : 41 - di(dimethylamino)benzophenone and p-tolyl-m-phenetidine is mixed with sulphamic acid, the mixture is treated with hot water and filtered and the sulphamate of the dyestuff is crystallized from the filtrate; its aqueous solution gives reddish blue shades on tannin-mordanted cotton; (5) the hydrochloride of the condensation product from 4 : 41 - di(dimethylamino)benzophenone and a :b - dinaphthylamine is mixed with ammonium sulphamate; an aqueous solution of the mixture gives greenish blue shades on tannin-mordanted cotton; (6) and (7) Methyl violet 2B base and Methyl violet R base are ground with sulphamic acid.
机译:通过将游离碱与氨基磺酸混合,或将游离碱的盐与氨基磺酸的盐混合,并根据需要干燥,或将游离碱转化为氨基磺酸盐,可使碱性着色剂易溶于水。氨基磺酸盐通过与氨基磺酸反应或使其盐与氨基磺酸的可溶性盐反应而得到。在实例中:(1)将罗丹明B基础粉末与粉末状氨基磺酸混合; (2)用氨基磺酸研磨维多利亚蓝B或R碱; (3)将A啶橙基础粉末与粉末状的氨基磺酸混合; (4)将4:41的缩合产物的游离碱-二(二甲基氨基)二苯甲酮和对甲苯基-间苯乙啶与氨基磺酸混合,将混合物用热水处理并过滤,将染料的氨基磺酸盐从滤液中结晶出来;其水溶液在单宁染色的棉布上产生红蓝色调。 (5)将4:41-二(二甲基氨基)二苯甲酮和:b-二萘胺的缩合产物的盐酸盐与氨基磺酸铵混合;混合物的水溶液在单宁染棉上产生绿色的蓝色阴影; (6)和(7)用氨基磺酸将甲基紫2B碱和甲基紫R碱研磨。

著录项

  • 公开/公告号GB495782A

    专利类型

  • 公开/公告日1938-11-18

    原文格式PDF

  • 申请/专利权人 MAX WYLER;IMPERIAL CHEMICAL INDUSTRIES LIMITED;

    申请/专利号GB19370013903

  • 发明设计人

    申请日1937-05-18

  • 分类号C09B67/32;

  • 国家 GB

  • 入库时间 2022-08-24 05:01:28

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