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An improved process for the extraction and purification of wax obtained from the flesh of sisal

机译:一种从剑麻果肉中提取和纯化蜡的改进方法

摘要

Purified sisal wax is obtained from sisal flesh by extraction with a hot organic solvent followed by treatment of the extract solution with an absorbent material which eliminates resinous matter, chlorophyll and other impurities, the purified wax being finally obtained from the clean extract solution by distilling off the solvent. The absorbent may be added to the extract solution in comminuted form and then removed by filtration or the extract solution may be percolated through a column of the absorbent. The solvents specified comprise hydrocarbons such as benzene, light petroleum, petroleum ether, chlorinated hydrocarbons such as trichlorethylene, alcohols such as ethyl alcohol and azeotropic mixtures such as benzene and ethyl alcohol azeotrope. The extraction of the sisal flesh may be effected under reflux or by repeated leachings of the material with hot solvent. The absorbent material specified comprises activated carbon, bone charcoal, alumina and bone meal. Specification 630,271 is referred to.
机译:通过用热的有机溶剂萃取从剑麻果肉中纯化出剑麻蜡,然后用一种吸收剂材料处理萃取液,该吸收剂材料消除了树脂质,叶绿素和其他杂质,最终通过蒸馏除去清洁的萃取液而获得了纯化蜡。溶剂。可以将吸收剂以粉碎的形式添加到提取液中,然后通过过滤除去,或者可以将提取液渗透通过吸收剂的柱。规定的溶剂包括烃,例如苯,轻石油,石油醚,氯化烃,例如三氯乙烯,醇(例如乙醇)和共沸混合物(例如苯和乙醇共沸物)。剑麻肉的提取可以在回流下或通过用热溶剂反复浸出材料来进行。指定的吸收性材料包括活性炭,骨炭,氧化铝和骨粉。参考规格630,271。

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