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methods for the extraction of isoprene using aqueous n formylmorfoline and / or morfoline.
methods for the extraction of isoprene using aqueous n formylmorfoline and / or morfoline.
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机译:甲酰吗啉和 /或吗啉水溶液萃取异戊二烯的方法。
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摘要
A multi-stage method is disclosed whereby isoprene of high purity is recovered from mixtures of C5 hydrocarbons containing it, wherein the mixture is subjected to a first extractive distillation stage in the presence of a solvent, such as morpholine and N-formyl-morpholine, containing water and in which olefinic and saturated hydrocarbons are withdrawn as a top product; a second extractive distillation stage effects the withdrawal of the major part of the cyclopentadiene and acetylene compounds present in the bottom product of the first stage as a sidestream and said solvent constitutes a bottom product for recycling to said first and second stage; in a third extractive distillation stage the top product of the second stage is treated with solvent containing water, fed to the third stage from a stripper and then recycled as bottom product to said stripper; and, in a rectification stage, isoprene of desired purity is recovered from the overhead product of the third extractive distillation stage.
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