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Method of separation of acrylic acid from the solutions in the phosphate of sorting butyl n - -
Method of separation of acrylic acid from the solutions in the phosphate of sorting butyl n - -
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机译:从正丁醇正丁酯的磷酸盐中分离溶液中丙烯酸的方法
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摘要
P the invention relates to the separation of acrylic acid from the solutions in the phosphate of sorting - n -. & / p & & p & the method consists of: a. to form a vapor phase comprising the acrylic acid and a part of the sorting - n - butyl by heating the starting solution, under conditions which avoid the degradation of the sorting - n - butyl, b and then, after partial or complete condensation of the vapor phase, to carry out, on the basis of this phase, a distillation of acrylic acid by maintaining in the bottom of the column, an acrylic acid content sufficient to avoid the degradation of the sorting - n - butyl in the operating conditions, c, optionally to be recycled to the supply of the stage a, the distillation residue of the stage b / p
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机译:本发明涉及在分选-n-的磷酸盐中从溶液中分离丙烯酸。 & / p> & &该方法包括:在避免分选-n-丁基降解的条件下,通过加热原料溶液,然后在部分或完全缩合缩合后,通过加热原料溶液,形成包含丙烯酸和部分分选-n-丁基的气相。气相,以在该相的基础上通过在塔底保持蒸馏来进行丙烯酸蒸馏,该丙烯酸含量足以避免分选的降解-在操作条件下,n-丁基,可选地再循环至阶段a的供应,阶段b / p <>的蒸馏残余物
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