首页> 外国专利> method for the separation of ursodesoxycholsaeure and chenodesoxycholsaeure and products obtained during the procedure.

method for the separation of ursodesoxycholsaeure and chenodesoxycholsaeure and products obtained during the procedure.

机译:分离熊去氧胆酸和鹅去氧胆酸的方法以及在该过程中获得的产物。

摘要

A mixture of ursodeoxycholic acid and of chenodeoxycholic acid as well as of their salts and esters is reacted with a silylating agent in a suitable anhydrous organic solvent; the corresponding silyl-derivatives thus obtained are separated by crystallization and pure ursodeoxycholic acid is recovered from the corresponding silyl-derivatives in the usual manner.
机译:熊去氧胆酸和鹅去氧胆酸的混合物以及它们的盐和酯在合适的无水有机溶剂中与甲硅烷基化剂反应。通过结晶分离由此得到的相应的甲硅烷基衍生物,并以常规方式从相应的甲硅烷基衍生物中回收纯的熊去氧胆酸。

著录项

  • 公开/公告号AT3641T

    专利类型

  • 公开/公告日1983-06-15

    原文格式PDF

  • 申请/专利权人 BLASINACHIM S.P.A.;

    申请/专利号AT19800103817T

  • 发明设计人 BONALDI ANTONIO;MOLINARI EGIDIO;

    申请日1980-07-04

  • 分类号C07J9/00;C07J51/00;

  • 国家 AT

  • 入库时间 2022-08-22 10:51:53

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