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PROCESS FOR THE SEPARATION OF PALLADIUM FROM THE PRODUCTS DERIVED FROM THE CARBONYLATION OF DIENES CONJUGATED IN THE PRESENCE OF PALLADIUM
PROCESS FOR THE SEPARATION OF PALLADIUM FROM THE PRODUCTS DERIVED FROM THE CARBONYLATION OF DIENES CONJUGATED IN THE PRESENCE OF PALLADIUM
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机译:从存在钯的共轭二烯的碳酰化反应中分离出钯的方法
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ABSTRACT OF THE DISCLOSURE: Process for separating palladium from the products of the carbonylation reaction of carbon monoxide conjugated dienes in the presence of an alcohol, a halogenated hydracid and a palladium catalyst, con-resistant to be contacting the products of the reac-tion carbonylation with a quaternary ammonium salt, quaternary phosphonium or quaternary arsonium, an alcohol and a hydrocarbon solvent apolar aliphatic or cycloaliphatic, and recovering after decantation palla-dium and quaternary onium salt in alcoholic solution and the products of the carbonylation reaction in hydrocarbon solution. This method has the prin cipal-advantage that the separated Pd is in alcoholic solution and can be recycled for a new opera-tion while retaining its activity.
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