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Preparation process of 1- (5-oxohexyl) -3,7-dimethyl tilxantina
Preparation process of 1- (5-oxohexyl) -3,7-dimethyl tilxantina
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机译:1-(5-氧己基)-3,7-二甲基多氧黄腐菌素的制备方法
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摘要
1-(5-Oxo-hexyl) 3,7-dimethyl xanthine of formula (I) is made by a phase transfer reaction between 3,7-dimethyl xanthine and 1-bromo 5-hexanone, with strong agitation in presence of a phase transfer catalyst, e.g. tetrabutyl ammonium hydrogen sulphate, at below b.pt.. The aq. phase is NaOH soln. and the organic phase is an immiscible solvent e.g. benzene.
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