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PRODUCTION OF 6-HALO-3-METHYL-1- TRIALKYLSILYLOXY-1, 3, 5-HEXATRIENE
PRODUCTION OF 6-HALO-3-METHYL-1- TRIALKYLSILYLOXY-1, 3, 5-HEXATRIENE
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机译:生产6-卤代-3-甲基-1-三乙氧基LY-1、3、5-己三烯
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摘要
1. Process for the preparation of a 6-halo-geno-3-methyl-1-trialkylsilyloxy-1,3,5-hexatrien of general formula : see diagramm : EP0242247,P4,F1 in which X denotes a halogen atom and R denotes an alkyl radical containing 1 to 4 carbon atoms, characterized in that a halosilane is reacted in the presence of a tertiary amine wiht a 6-hal-3-methyl-3,5-hexadienal, the operation being carried out in an inert organic solvent at a temperature of between -10 and +30 degrees C.
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