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Method of introduction of samples in a gas chromatograph and device for implementing it.

机译:在气相色谱仪中引入样品的方法及其实施装置。

摘要

Specimens are introduced into a gas chromatograph via the evaporator as follows. The specimen carrier (2) is connected to the evaporator (1) only for sufficient time for transfer of the specimen to the evaporator. The vapour obtained by evapn. of the specimen in the evaporator flows through a throttle (15) of constant cross-section into the chromatograph column. When this flow has ceased, the evaporator (1) is connected to atmos. The volume of the specimen carrier is rather smaller than that of the evaporator and the pressure generated by evapn. expels the vapours from the evaporator into the carrier gas stream flowing into the column. The vapours are transferred from the evaporator into the column by the carrier gas stream, which is fed into the evaporator. After the vapours have been transferred into the column, the feed of carrier gas is interrupted and shifted to the inlet to the column behind the outlet from the throttle.
机译:样品如下通过蒸发器被引入气相色谱仪中。样本载体(2)仅与蒸发器(1)连接足够的时间,以将样本转移至蒸发器。蒸发得到的蒸气。蒸发器中的样品中的一部分通过恒定横截面的节流阀(15)流入色谱柱。当该流停止时,蒸发器(1)连接到atmos。样品载体的体积比蒸发器的体积小,蒸发所产生的压力也要小。将蒸气从蒸发器中排入流入塔中的载气流中。蒸气通过载气流从蒸发器转移到塔中,该载气流被供给到蒸发器中。蒸气转移到色谱柱后,载气的进料被中断并转移到节流阀出口后面色谱柱的入口。

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