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Method and device for the introduction of a sample into a gas chromatograph

机译:将样品引入气相色谱仪的方法和装置

摘要

There is provided a method for sample introduction into a gas chromatograph for performing sample analysis, in which a sample is introduced into a removable sample container, the container is placed in a sample introduction device, the device with said container is inserted into a gas chromatograph injector, and the sample is then vaporized for effecting analysis thereof by the gas chromatograph. The non-volatile residues of the sample retained in the container after vaporization and are removed with the container prior to performing the next analysis. There is also provided a method for direct sample introduction into a mass spectrometer for performing sample analysis, in which a sample is loaded into a sample container, the container with the sample is introduced into the injector of a gas chromatograph connected to a mass spectrometer through a capillary column, the injector is heated to a temperature sufficient to vaporize the sample to produce a flow of compounds which are swept to the mass spectrometer by a carrier gas, and the container is removed from the injector prior to performing the next analysis. Devices for introducing samples into a gas chromatograph for analyzing said sample are also described and claimed.
机译:提供了一种用于将样品引入气相色谱仪以进行样品分析的方法,其中将样品引入可移动样品容器中,将容器放置在样品引入装置中,将具有所述容器的装置插入气相色谱仪中然后,将样品蒸发,然后通过气相色谱仪对其进行分析。样品在蒸发后保留在容器中的非挥发性残留物,并在进行下一次分析之前与容器一起除去。还提供了一种将样品直接引入质谱仪中进行样品分析的方法,其中将样品装入样品容器中,将装有样品的容器引入气相色谱仪的进样器中,该进样器通过以下方式与质谱仪连接在毛细管柱中,将进样器加热到足以蒸发样品的温度,以产生化合物流,这些化合物流被载气吹扫到质谱仪中,在执行下一个分析之前,将容器从进样器中取出。还描述并要求保护了将样品引入气相色谱仪中以分析所述样品的装置。

著录项

  • 公开/公告号US5686656A

    专利类型

  • 公开/公告日1997-11-11

    原文格式PDF

  • 申请/专利权人 AMIRAV;AVIV;

    申请/专利号US19960607474

  • 发明设计人 AVIV AMIRAV;SHAI DAGAN;

    申请日1996-02-27

  • 分类号G01N30/02;

  • 国家 US

  • 入库时间 2022-08-22 02:41:09

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