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Apparatus for overpressured thin-layer chromatographic technique

机译:超压薄层色谱技术的仪器

摘要

The invention relates to an apparatus for overpressured thin- layer chromatographic technique, comprising at least one carrier plate arranged adjacent a closed space, a sorbent layer arranged on the surface of said carrier plate, means for covering the surface of said sorbent layer under influence of overpressure generated in said closed space, a first inlet for admitting solvent to said sorbent layer, a second inlet for admitting overpressurizing medium into said closed space, a heating unit for altering temperature of said sorbent layer and a temperature control unit for energizing said heating unit. The apparatus according to the invention ensures improved efficiency of the chromatographic developments carried out under overpressure. By means of the apparatus chromatograms can be obtained with increasing speed of separation.
机译:本发明涉及一种用于超压薄层色谱技术的设备,该设备包括至少一个邻近封闭空间布置的载板,布置在所述载板表面上的吸附剂层,在压力的影响下覆盖所述吸附剂层表面的装置。在所述封闭空间中产生超压,使溶剂进入所述吸附剂层的第一入口,使超压介质进入所述封闭空间的第二入口,用于改变所述吸附剂层的温度的加热单元和为所述加热单元供能的温度控制单元。根据本发明的设备确保了在超压下进行的色谱展开的改进的效率。借助于该装置,可以以增加的分离速度获得色谱图。

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