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Alpha-alumina in the form of spherical non-aggregated particles having a narrow size distribution and sizes below 2 microns and process for preparing same

机译:具有窄的尺寸分布和小于2微米的尺寸的球形非聚集颗粒形式的α-氧化铝及其制备方法

摘要

Alpha-alumina consisting essentially of solid, spherical, non- aggregated particles, having a diameter from 0.06 to 2 m, a polydispersion index below 2.0, a total porosity below 0.3 cc/g, a specific surface area from 0.7 to 80 m.sup.2 /g, and an apparent density of the particles from 3.20 to 3.94 g/cm.sup.3. The alpha-alumina is prepared by a process consisting, in that an alpha-alumina precursor, having a water content from 2 to 33% by weight, at starting temperatures ranging from room temperature to 850 C., and consisting essentially of solid spherical, non-aggregated particles, having a particle diameter from 0.07 to 2.3 m and a polydispersion index of . ltoreq.2.0, is subjected to a heat-treatment at temperatures ranging from 1130 to 1700 C., said precursor being instantaneously brought from the starting temperature to the treatment temperature, and by carrying out the treatment during times, as generally indicated in the accompanying FIG. 1 between straight lines (a) and (b), which are sufficient to convert the precursor to phase alpha, but not such as to cause breakages and/or aggregations; the resulting product being then brought again to room temperature by means of a non-instantaneous cooling of the order of at least 10 seconds.
机译:α-氧化铝主要由直径为0.06至2 m的固体球形非聚集颗粒组成,多分散指数低于2.0,总孔隙率低于0.3 cc / g,比表面积为0.7至80 m。 0.2 / g,颗粒的表观密度为3.20至3.94 g / cm 3。 α-氧化铝的制备方法是,在室温至850℃的起始温度下,水含量为2-33%(重量)的α-氧化铝前体基本上由固体球形,非聚集颗粒,粒径为0.07至2.3 m,多分散指数为。将ltoreq.2.0在1130至1700℃的温度范围内进行热处理,所述前体立即从起始温度升至处理温度,并在一段时间内进行处理,如随附附图中通常所示图。在直线(a)和(b)之间的1,足以将前体转化为相α,但不足以引起断裂和/或聚集;然后通过至少约10秒的非瞬时冷却使所得产物再次回到室温。

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