首页> 外国专利> PREPARATION OF RAW MATERIAL POWDER FOR READILY SINTERABLE HIGH-TEMPERATURE SUPERCONDUCTING CERAMIC

PREPARATION OF RAW MATERIAL POWDER FOR READILY SINTERABLE HIGH-TEMPERATURE SUPERCONDUCTING CERAMIC

机译:原始可烧结高温超导陶瓷粉末的制备

摘要

PURPOSE:To obtain the title readily sinterable powder capable of giving dense superconductors of high critical current density by adding a copper compound solution followed by a precipitating agent to a coprecipitate made up of a rare earth element component and alkaline earth element component to form a three-component coprecipitate which is then calcined. CONSTITUTION:Firstly, a solution of a rare earth element compound (e.g., YCl3), a second solution of an alkaline earth element compound (e.g., BaCl2) and a precipitating agent (e.g., ammonia water) are mutually mixed to form a coprecipitate made up of a rare earth element component and an alkaline earth element component. Second, a solution of a copper compound (e.g., copper nitrate) is added to the above coprecipitate to prepare a suspension, which is then spiked with a precipitation-forming agent (e.g., oxalic acid) to produce a coprecipitate made up of a rare earth element component, an alkaline earth element component and a copper component. Thence, this coprecipitate is calcined at 500-950 deg.C to obtain the objective readily sinterable raw material powder for rare earth element-alkaline earth element-copper oxide-based high- temperature superconducting ceramics.
机译:用途:为了获得标题易于烧结的粉末,该粉末可通过向由稀土元素组分和碱土元素组分组成的共沉淀物中加入铜化合物溶液和沉淀剂,从而提供高临界电流密度的致密超导体,从而形成三种组分共沉淀,然后进行煅烧。组成:首先,将稀土元素化合物(例如YCl3)的溶液,第二种碱土元素化合物(例如BaCl2)的溶液和沉淀剂(例如氨水)相互混合以形成共沉淀物。由稀土元素成分和碱土元素成分组成。其次,将铜化合物(例如硝酸铜)的溶液添加到上述共沉淀物中以制备悬浮液,然后将其与沉淀形成剂(例如草酸)掺混以产生由稀有物组成的共沉淀物。土元素成分,碱土金属元素成分和铜成分。因此,将该共沉淀物在500-950℃下煅烧以获得用于稀土元素-碱土金属元素-铜氧化物基高温超导陶瓷的目标易烧结原料粉末。

著录项

  • 公开/公告号JPH0222124A

    专利类型

  • 公开/公告日1990-01-25

    原文格式PDF

  • 申请/专利权人 UBE IND LTD;

    申请/专利号JP19870315386

  • 发明设计人 MIURA HIROSHI;ITO KOSUKE;ODAN KYOJI;

    申请日1987-12-15

  • 分类号C04B35/00;C01G1/00;C01G3/00;C04B35/45;H01B13/00;

  • 国家 JP

  • 入库时间 2022-08-22 06:25:16

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