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INDUCTIVELY-COUPLED PLASMA MASS SPECTROMETRIC APPARATUS

机译:电感耦合等离子体质谱仪

摘要

PURPOSE:To prevent cations from being detected as background spectra and to enhance the accuracy of analysis by disposing a cation column which removes the cation between constant flow rate pumps and a sampling valve. CONSTITUTION:The cation column 9 which removes cations is provided between the constant flow rate pumps 2, 7 and the sampling valve 3. The carrier soln. in a carrier soln. tank 6 is sent through a pump 7 the column 9 a 5th connecting port 3e of the sampling value 3 a 4th connecting port 3d to a nebulizer 8' when the pump 7 is driven. The cations contained in the carrier soln. and the cations eluted from the wetting members of the pump 7 are removed during the passage through the column 9 and are prevented from arriving at the nebulizer 8'. Such a phenomenon that the cations contained in the carrier soln. and the cations eluted from the wetting members of the pump 7 are detected as the background spectra and that the degradation of the lower detection limit of the elements to be measured is degraded to degrade the accuracy of measurement is obviated.
机译:目的:为防止阳离子被检测为背景光谱,并通过设置阳离子柱来去除分析仪的准确性,该柱可去除恒流泵和进样阀之间的阳离子。组成:用于去除阳离子的阳离子塔9位于恒流泵2、7和采样阀3之间。在载体溶液中。当泵7被驱动时,罐6通过泵7被送至柱9a,采样值3的第五连接端口3e,第四连接端口3d到喷雾器8'。载剂溶液中包含的阳离子。并且,从泵7的湿润部件上溶出的阳离子在通过柱9的过程中被除去,并被阻止到达雾化器8'。这种现象使载体中的阳离子溶解。并且,检测从泵7的湿润部件溶出的阳离子作为背景光谱,并且能够避免被测定元素的检测下限的降低而降低测量精度。

著录项

  • 公开/公告号JPH01304352A

    专利类型

  • 公开/公告日1989-12-07

    原文格式PDF

  • 申请/专利权人 YOKOGAWA ELECTRIC CORP;

    申请/专利号JP19880134145

  • 发明设计人 NAGAO TAKEO;KISHI YOKO;

    申请日1988-05-31

  • 分类号G01N27/62;G01N30/02;G01N30/72;G01N30/84;H01J49/04;

  • 国家 JP

  • 入库时间 2022-08-22 06:20:36

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