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CONTINUOUS PROCESS FOR THE PRODUCTION OF SOLID CALCIUM PHOSPHATES FROM RAW PHOSPHATE WITHOUT THE ADDITION OF PHOSPHORIC ACID AND LIME
CONTINUOUS PROCESS FOR THE PRODUCTION OF SOLID CALCIUM PHOSPHATES FROM RAW PHOSPHATE WITHOUT THE ADDITION OF PHOSPHORIC ACID AND LIME
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机译:在不添加磷酸和石灰的情况下从原始磷酸盐生产固体磷酸钙的连续过程
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Solid calcium phosphates are prepd. in a continuous process from raw phosphates without the addn. of ether-phosphoric acid or lime. 50-200 g raw phosphate is dissolved in 1l of processing acid contg. 100-750g P2O5 and 0-80g CaO. The soln is agitated for 20 mins.-6 hrs. at 20-120 deg.C. When mono-calcium phosphate is prepd. the processing acid contains 0-5 wt% CaO and 35-75 wt% P2O5. Any sediment is filtered out. The soln. is cooled and mono-sodium phosphate is sepd. by filtration. For the prepn of di:calcium-phosphate the process acid contains 0-8 wt% CaO and 5-35 wt.% P2O5. The prod. is filtered out. Mixed phosphates are prepd from process acid, which contains 1-5 wt% CaO and 25-40 wt% P2O5. the prod is filtered out. - In all three cases any excess calcium-over and above that, stoichiometrically necessary for the prepn of a cpd. in the next cycle-is removed from the filtrate, and the filtrate is then recirculated as process-acid.
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