METHOD OF PRODUCING MANGANESE DICYCLOPENTDIENIDE OR MANGANESE BIS(METHYLCYCLOPENTADIENIDE)

摘要

the invention u043eu0442u043du043eu0441u0438u0442u0441u00a0 to u043cu0435u0442u0430u043bu043bu043eu043eu0440u0433u0430u043du0438u0447u0435u0441u043au0438u043c u0441u043eu0435u0434u0438u043du0435u043du0438u00a0u043c, in particular to obtain u0434u0438u0446u0438u043au043bu043eu043fu0435u043du0442u0430u0434u0438u0435u043du0438u0434u0430 manganese or bis (u043cu0435u0442u0438u043bu0446u0438u043au043bu043eu043fu0435u043du0442u0430u0434u0438u0435u043du0438u0434u0430) of manganese, which e can be used as u0430u043du0442u0438u0434u0435u0442u043eu043du0430u0442u043eu0440u043eu0432. the objective is to reduce the process cost and improving the process of trust product by current.synthesis of lead u044du043bu0435u043au0442u0440u043eu043bu0438u0437u043eu043c u0446u0438u043au043bu043eu043fu0435u043du0442u0430u0434u0438u0435u043du0438u0434u0430 u043du0430u0442u0440u0438u00a0 or u043cu0435u0442u0438u043bu0446u0438u043au043bu043eu043fu0435u043du0442u0430u0434u0438u0435u043du0438u0434u0430 u043du0430u0442u0440u0438u00a0 using manganese electrodes in a mixture of liquid ammonia with u043eu0440u0433u0430u043du0438u0447 u0435u0441u043au0438u043c aether, for example u0442u0435u0442u0440u0430u0433u0438u0434u0440u043eu0444u0443u0440u0430u043du043eu043c or u0434u0438u043cu0435u0442u0438u043bu043eu0432u044bu043c ether u0434u0438u044du0442u0438u043bu0435u043du0433u043bu0438u043au043eu043bu00a0 (1: 1) at 20 40u0441, current density of 0.05, 0.10 and / cm2 and u043du0430u043fu0440u00a0u0436u0435u043du0438u0438 in the bathtub 5 - 10.these u0443u0441u043bu043eu0432u0438u00a0 increases the output of target substances from 3 to 25 to 80 - 83% decline in u043du0430u043fu0440u00a0u0436u0435u043du0438u00a0 at bath with 20 - 30 to 5 - 10. 2, table 2).