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Preparation of high uniformity polycrystalline ceramics by presintering, hot isostatic pressing and sintering and the resulting ceramic

机译:通过预烧结,热等静压和烧结制备高均匀度的多晶陶瓷以及所得的陶瓷

摘要

Polycrystalline ceramic bodies having uniform transparent optical characteristics are produced by providing a green compact, presintering that compact at a temperature in the range from about 1, 350° C. to about 1,650° C. until the closed porosity stage is reached, hot isostatic pressing the presintered compact to collapse substantially all pores disposed at grain boundaries and resintering the hot isostatically pressed compact at a temperature in the range from 1, 700° C.-1,950. degree. C. to cause grain growth under conditions in which pores, within those grains which are consumed by the growth of other grains, collapse as the grain boundary of the growing grain passes through the location of the pore in the smaller grain being consumed.
机译:通过提供生坯,在约1,350℃至约1,650℃范围内的温度下进行预烧结,直至达到闭合孔隙阶段,进行热等静压,从而制备具有均匀透明光学特性的多晶陶瓷体。该预烧结的压坯使基本上所有位于晶界处的孔塌陷并在1,700°C-1,950的温度范围内对热等静压的压坯进行树脂处理。度。 C.引起晶粒生长的条件是,随着其他晶粒的生长而消耗的那些晶粒内的孔随着生长晶粒的晶界穿过被消耗的较小晶粒中的孔的位置而塌陷。

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