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PRODUCTION OF HIGH-PURITY KAOLINITE-LIKE MINERAL

机译:高纯度高岭土类矿物的生产

摘要

PURPOSE:To obtain a high-purity kaolinite-like mineral containing neither impurities nor unreacted substances in production by hydrothermal synthesis by blending an aqueous solution of sodium silicate with an aqueous solution of aluminum sulfate at a specific pH, subjecting Na ion to ion exchange for proton to give a gel and using the gel as a raw material. CONSTITUTION:An aqueous solution of sodium silicate is uniformly blended with an aqueous solution of aluminum sulfate while maintaining at pH 4-12 to give a mixed gel of silica and alumina. Then, Na in the gel is subjected to ion exchange for proton by using a cationic exchanging ion exchange resin containing a sulfonic group or carboxylic group as a functional group. Then, the prepared raw material gel is fed to an autoclave so as to give 5wt.% slurry concentration, subjected to hydrothermal treatment at 220 deg.C for 10 days, cooled, washed with water, filtered and dried to give a kaolinite-like mineral, a reaction product.
机译:用途:通过在特定pH下将硅酸钠水溶液与硫酸铝水溶液混合,然后对Na离子进行离子交换,以进行水热合成,以生产高纯度的不含杂质或未反应物质的类高岭石矿物。质子产生凝胶,并以凝胶为原料。组成:将硅酸钠水溶液与硫酸铝水溶液均匀混合,同时保持pH 4-12,得到二氧化硅和氧化铝的混合凝胶。然后,通过使用含有磺酸基或羧基作为官能团的阳离子交换离子交换树脂,对凝胶中的Na进行质子的离子交换。然后,将制备的原料凝胶进料到高压釜中以得到5wt。%的浆料浓度,在220℃下进行水热处理10天,冷却,用水洗涤,过滤并干燥以得到高岭石状。矿物,一种反应产物。

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