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Electrothermal direct injection torch for inductively coupled plasma

机译:电热直喷炬用于电感耦合等离子体

摘要

An inductively coupled plasma spectroscopy apparatus is provided in which an inductively coupled plasma torch and an analyte sample atomizer are integrally formed as a single unit. The atomizer portion of the apparatus includes two electrodes and a plasma nozzle through which a heating element is placed. Test samples may be placed into a sample vessel which is positioned within the heating element. The torch portion includes a glass containment wall surrounding at least a portion of the plasma nozzle to define a plasma chamber located immediately adjacent to the sample vessel. The glass containment wall contains a radio frequency (RF) coil wrapped about its periphery which is inductively coupled to a supply of gas. A variable rate cooling manifold is also provided about the periphery of the containment wall. The integral design effectively reduces the buildup of memory condensate within the apparatus, thereby decreasing contamination and improving the sensitivity of the results obtained.
机译:提供了一种感应耦合等离子体光谱装置,其中感应耦合等离子体炬和分析物样品雾化器一体地形成为单个单元。该设备的雾化器部分包括两个电极和等离子喷嘴,通过该等离子喷嘴放置加热元件。可以将测试样品放入位于加热元件内的样品容器中。割炬部分包括玻璃容器壁,该玻璃容器壁围绕等离子体喷嘴的至少一部分以限定紧邻样品容器的位置的等离子体室。玻璃隔离墙包含一个缠绕在其外围的射频(RF)线圈,该线圈感应耦合至气体供应。围绕安全壳壁的外围还设置了可变速率的冷却歧管。整体设计有效地减少了设备中内存冷凝物的堆积,从而减少了污染并提高了所得结果的敏感性。

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