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production of vitamin d2 and vitamin d3 or active vitamin d2 and active vitamin d3 or its derivatives.
production of vitamin d2 and vitamin d3 or active vitamin d2 and active vitamin d3 or its derivatives.
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机译:生产维生素d2和维生素d3或活性维生素d2和活性维生素d3或其衍生物。
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摘要
Vitamin D2 and Vitamin D3 derivs of formula (I) (where R is H or Me; R3 is H or a hydroxyl-protecting gp; X and Y are H, 0H or a derivatised 0H; broken line is a single bond or (if R=H) a double bond); are produced from the 7,8-dihydroxy derivs of formula (II) (where R1 and R2 are H or a hydroxyl-protecting gp) by reductive elimination via the cyclic orthoester or thiocarbonate on the 7,8-hydroxyl gps, or by elimination using a reductive metal such as Ti.
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