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Method for determining tributyl phosphate and / or butanol by liquid chromatography

机译:液相色谱法测定磷酸三丁酯和/或丁醇的方法

摘要

The invention relates to the determination of tributyl phosphate (TBP) and / or butanol by liquid chromatography. BR/ A sample of an organic solution comprising TBP and / or butanol is injected into a column (1) filled with a polar solid stationary phase, for example of silica grafted with NH 2 groups, and covered by a mobile liquid phase of apolar nature, for example a mixture of heptane and ethyl acetate, from (9) and the TBP and / or butanol leaving the column is detected by refractometry in (11). / P
机译:本发明涉及通过液相色谱法测定磷酸三丁酯(TBP)和/或丁醇。
将包含TBP和/或丁醇的有机溶液样品注入到装有极性固体固定相(例如接有NH 2基团的二氧化硅的极性固相)的柱(1)中,并用非极性性质,例如(9)中的庚烷和乙酸乙酯的混合物,以及离开色谱柱的TBP和/或丁醇,通过(11)中的折光法检测。

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