首页> 外国专利> PROCEDURE FOR THE PREPARATION OF A CU/CO(ZN)/AI CATALYST FOR THE PRODUCTION OF C1-C6 ALCOHOLS FROM SYNTHESISED GAS AND THE CATALYST OBTAINED FROM SAID PROCEDURE

PROCEDURE FOR THE PREPARATION OF A CU/CO(ZN)/AI CATALYST FOR THE PRODUCTION OF C1-C6 ALCOHOLS FROM SYNTHESISED GAS AND THE CATALYST OBTAINED FROM SAID PROCEDURE

机译:从合成气中制备CU / CO(ZN)/ Al催化剂以生产C1-C6醇的方法以及从所述方法中获得的催化剂

摘要

Process for the preparation of Catalysts by complexation method especially applicable When The Catalyst formulations contain elements of Group VIII or IB comprisingS: stages of Dissolution in Water of the metal ions are in the form of Nitrate; temperature of the complex Agent added to the aqueous solution of metal ions; EvaporationThe aqueous Solvent to obtain a Solution Concentrated Viscose; Vacuum Oven Drying the concentrated solution to obtain a solid with the appearance of a colored decomp Rigid foam;Solid osition with programmed temperature in atmosphere of n2 from room temperature up to 280 * C using heating rates under 2 * C / min in air temperature Warming Program;Ada until 500 * C previously Decomposed precursor in N2.And subsequent calcination in air at 500 * C for 8h; The complexing Agent is a multifunctional Organic hydroxy acid of no more than six carbon ATOMS, the type of the acids Citric, lactic,Tartaric, Malic acid or Glycolic Acid in a ratio of 2, 5 - 0 5g EP, EP acid / g of total metal ions.
机译:通过络合方法制备催化剂的方法,特别适用于以下情况:当催化剂配方中含有VIII或IB族元素时,包括S:金属离子在水中的溶解阶段为硝酸盐形式;添加到金属离子水溶液中的络合剂的温度;蒸发在水性溶剂中获得溶液浓缩的粘胶;真空烤箱干燥浓缩的溶液,得到具有彩色反腐刚性泡沫的固体;在程序设定温度下,在n2气氛中从室温到280 * C进行固溶,加热速率为2 * C / min,在空气温度下升温程序; Ada直到500 * C之前在N2中分解,然后在空气中于500 * C煅烧8h;络合剂是不超过6个碳原子的ATOMS多功能有机羟基酸,柠檬酸,乳酸,酒石酸,苹果酸或乙醇酸的比例为2、5-5 5 g EP,EP酸/ g总金属离子。

著录项

  • 公开/公告号AR247834A1

    专利类型

  • 公开/公告日1995-04-28

    原文格式PDF

  • 申请/专利权人 YPF S.A.;

    申请/专利号AR19930324652

  • 发明设计人

    申请日1993-04-01

  • 分类号B01J23/76;B01J37/08;

  • 国家 AR

  • 入库时间 2022-08-22 04:20:30

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