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PROCEDURE FOR THE PREPARATION OF A CU/CO(ZN)/AI CATALYST FOR THE PRODUCTION OF C1-C6 ALCOHOLS FROM SYNTHESISED GAS AND THE CATALYST OBTAINED FROM SAID PROCEDURE
PROCEDURE FOR THE PREPARATION OF A CU/CO(ZN)/AI CATALYST FOR THE PRODUCTION OF C1-C6 ALCOHOLS FROM SYNTHESISED GAS AND THE CATALYST OBTAINED FROM SAID PROCEDURE
Process for the preparation of Catalysts by complexation method especially applicable When The Catalyst formulations contain elements of Group VIII or IB comprisingS: stages of Dissolution in Water of the metal ions are in the form of Nitrate; temperature of the complex Agent added to the aqueous solution of metal ions; EvaporationThe aqueous Solvent to obtain a Solution Concentrated Viscose; Vacuum Oven Drying the concentrated solution to obtain a solid with the appearance of a colored decomp Rigid foam;Solid osition with programmed temperature in atmosphere of n2 from room temperature up to 280 * C using heating rates under 2 * C / min in air temperature Warming Program;Ada until 500 * C previously Decomposed precursor in N2.And subsequent calcination in air at 500 * C for 8h; The complexing Agent is a multifunctional Organic hydroxy acid of no more than six carbon ATOMS, the type of the acids Citric, lactic,Tartaric, Malic acid or Glycolic Acid in a ratio of 2, 5 - 0 5g EP, EP acid / g of total metal ions.
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机译:通过络合方法制备催化剂的方法,特别适用于以下情况:当催化剂配方中含有VIII或IB族元素时,包括S:金属离子在水中的溶解阶段为硝酸盐形式;添加到金属离子水溶液中的络合剂的温度;蒸发在水性溶剂中获得溶液浓缩的粘胶;真空烤箱干燥浓缩的溶液,得到具有彩色反腐刚性泡沫的固体;在程序设定温度下,在n2气氛中从室温到280 * C进行固溶,加热速率为2 * C / min,在空气温度下升温程序; Ada直到500 * C之前在N2中分解,然后在空气中于500 * C煅烧8h;络合剂是不超过6个碳原子的ATOMS多功能有机羟基酸,柠檬酸,乳酸,酒石酸,苹果酸或乙醇酸的比例为2、5-5 5 g EP,EP酸/ g总金属离子。
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