首页>
外国专利>
Process for the preparation of 9,9-bis-(4-hydroxyphenyl)fluorene
Process for the preparation of 9,9-bis-(4-hydroxyphenyl)fluorene
展开▼
机译:制备9,9-双-(4-羟苯基)芴的方法
展开▼
页面导航
摘要
著录项
相似文献
摘要
A polyalkylene glycol is added to a reaction mixture obtained by a condensation reaction of fluorenone with phenol in the presence of ss-mercaptopropionic acid and HCl gas, excess phenol is then distilled off, and the residue is crystallised out from a solvent which is miscible with the polyalkylene glycol used. After recrystallisation and treatment with water, 9,9-bis-(4-hydroxyphenyl)fluorene is obtained in the form of a white crystalline product in a purity of above 99%.
展开▼