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METHOD OF SYNTHESIS OF AMINOPHENYLPERFLUOROALKYLSULFIDES
METHOD OF SYNTHESIS OF AMINOPHENYLPERFLUOROALKYLSULFIDES
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机译:合成氨基苯酚全氟烷基酯的方法
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摘要
FIELD: chemical technology. SUBSTANCE: synthesis is carried out by treatment of corresponding dinitrodiphenyldisulfides with alkaline or alkaline-earth metal in liquid ammonia and the following UV-irradiation of solution formed together with perfluoroalkyl iodide added to it. Under these conditions the yield of the end product is increased from 50-60 to 75-85%. Stages of isolation and purification of hazard aminothiophenols were excluded. EFFECT: increased yield of products, development of universal and safety method of synthesis. 2 tbl
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