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DISSOLVED METHYLLITHIUM-CONTAINING COMPOSITION FOR USE IN SYNTHESIS REACTIONS
DISSOLVED METHYLLITHIUM-CONTAINING COMPOSITION FOR USE IN SYNTHESIS REACTIONS
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机译:用于合成反应的溶解的含甲基甲硅烷基的组合物
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摘要
This invention relates to a dissolved methyllithium-containing composition for use in synthesis reactions (synthesis composition) and to processes of preparing the composition. In the synthesis composition the methyllithium is contained in a solvent of the general formula I IMG wherein R1 and R2 are independently a hydrogen, methyl or ethyl residue and R3 and R4 are a methyl or ethyl residue. To prepare the methyllithium-containing synthesis composition in accordance with the invention a) lithium powder or granular lithium is dispersed in a sol vent having the general formula I and methyl halide is added at a controlled rate, b) the reaction temperature is kept in the range form 0 to 60.degree.C, and c) the resulting lithium halide is separated from the methyl lithium solution.
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