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PRODUCTION OF YTTRIUM OXIDE FINE POWDER

机译:氧化钇细粉的生产

摘要

PROBLEM TO BE SOLVED: To obtain a yttrium fine powder excellent in sintering property, reactivity and dispersing property and suitable as a sintering raw material, a sintering assistant, a phosphor raw material, a catalyst or the like. ;SOLUTION: The yttrium oxide fine powder having 0.01-0.2μm primary particle diameter is produced by neutralizing an acidic base aq. solution of yttrium with a carbonate-containing basic salt aq. solution to ≥pH4 and to equal to or below a value generating a plate like crystal to precipitate yttrium carbonate, aging for ≥10hr while mixing at ≤50°C and firing the yttrium carbonate at 700-1300°C. The yttrium oxide fine powder fine in primary particle diameter, free from aggregated particle and having high quality is obtained.;COPYRIGHT: (C)1997,JPO
机译:解决的问题:获得烧结性,反应性和分散性优异并且适合作为烧结原料的钇细粉,烧结助剂,荧光体原料,催化剂等。 ;解决方案:通过中和酸性碱水溶液,制备一次粒径为0.01-0.2μm的氧化钇细粉。含碳酸盐碱性盐水溶液的钇溶液。溶液的pH值≥4,并且等于或低于此值,会生成类似晶体的板状沉淀物,从而沉淀出碳酸钇,在≤50°C混合时老化≥10hr,然后在700-1300°C烧制碳酸钇。获得一次粒径细,无聚集颗粒且质量高的氧化钇细粉。; COPYRIGHT:(C)1997,JPO

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