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Liquid phase grain growth method and liquid phase grain growth device

机译:液相晶粒生长方法和液相晶粒生长装置

摘要

PURPOSE: To increase the rate of a crystal growth by taking a solvent in a vessel, heating the solvent by a radiant heat from a heater positioned at the outside of the vessel and blocking the radiant heat from the heater at the circumference of the crystal precipitating part. ;CONSTITUTION: This method for a liquid phase crystal growing comprises loading a polycrystalline II-VI group compound such as ZnSe as a source crystal 2 and a Se-Te mixture as a solvent 3 into a crystal growing vessel 1, evacuating the inside of the crystal growing vessel 1 to a high vacuum while keeping the source crystal 2 by a difference in level K and sealing the open end of the vessel, then winding a radiant heat blocking material 9 directly and cylindrically on the upper surface of a heat sink 6 made of carbon, etc., and on the wall surface of the vessel 1 at the circumference of the crystal precipitating part while making the upper surface of a seed crystal 5 as a center, placing and heating the vessel in an electric furnace made by winding a heater 8 around a furnace core tube 7 to dissolve the source crystal 2 until its saturation in the solvent 3, transferring it by diffusion to a low temperature part caused by the reduction of the radiant heat to make the state of a supersaturation for growing crystal in contact with the seed crystal to obtain a single crystal at a large crystal growth rate.;COPYRIGHT: (C)1996,JPO
机译:目的:通过将溶剂放入容器中,通过来自位于容器外部的加热器的辐射热加热溶剂,并阻止晶体沉淀周围加热器的辐射热,以提高晶体的生长速率部分。 ;组成:这种用于液相晶体生长的方法包括将多晶II-VI基化合物(例如ZnSe作为源晶体2和Se-Te混合物作为溶剂3)装入晶体生长容器1中,排空晶体内部。晶体生长容器1处于高真空状态,同时保持源晶体2的高度差K并密封容器的开口端,然后将辐射热阻挡材料9直接和圆柱形地缠绕在制成的散热器6的上表面上在以晶种5的上表面为中心的同时,在容器1的壁上在晶体沉淀部分的圆周上的壁上放置碳,碳等,并且将容器放置在通过加热而卷绕的电炉中并加热围绕炉芯管7的加热器8将源晶体2溶解,直到其在溶剂3中饱和,然后通过扩散将其转移到由辐射热的减少引起的低温部分,从而形成过剩状态。晶体生长与晶种接触的取向,以大的晶体生长速率获得单晶。;版权所有:(C)1996,日本特许厅

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