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Process for the preparation of silica slurry for particle growth of pyrolytic silica nuclei and silica particles prepared by this process

机译:制备用于热解二氧化硅核的颗粒生长的二氧化硅浆料的方法以及通过该方法制备的二氧化硅颗粒

摘要

The present invention relates to a method for producing silica slurry for particle growth of pyrolytic silica nuclei, which is improved in shape irregularity and size limitation by using tetraethylorthosilicate (hereinafter referred to as 'TEOS') and hydrolysis and condensation polymerization of water. To silica particles prepared by the method. The present manufacturing method includes a step of dissolving the nuclei of the pyrolyzed silica particles produced by the vapor phase method in an alcohol in a basic atmosphere, and a step of reacting TEOS with water. Accordingly, the weight fraction (5 to 10 wt%) can be raised by growing TEOS by hydrolysis and polycondensation reaction with water using pyrolytic silica, which is relatively inexpensive and widely commercialized, as nuclei, It is possible to economically manufacture spherical silica particles having a very uniform and high purity.
机译:本发明涉及制备用于热解二氧化硅核的颗粒生长的二氧化硅浆料的方法,该方法通过使用原硅酸四乙酯(以下称为“ TEOS”)和水的水解和缩聚来改善形状不规则性和尺寸限制。以二氧化硅颗粒制备的方法。本制造方法包括在碱性气氛中将通过气相法制得的热解二氧化硅颗粒的核溶解在醇中的步骤,以及使TEOS与水反应的步骤。因此,通过使用相对廉价且被广泛商业化的热解二氧化硅,通过与水的水解和缩聚反应使TEOS与水反应来生长,可以提高重量分数(5〜10重量%),可以经济地制造具有以下性质的球形二氧化硅粒子。非常均匀和高纯度。

著录项

  • 公开/公告号KR19980071914A

    专利类型

  • 公开/公告日1998-10-26

    原文格式PDF

  • 申请/专利权人 이병구;

    申请/专利号KR19980026544

  • 发明设计人 이병구;

    申请日1998-07-02

  • 分类号C01B33/133;

  • 国家 KR

  • 入库时间 2022-08-22 02:47:39

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