首页> 外国专利> METHOD AND INSTALLATION FOR PRODUCING INTERMEDIATE PRODUCTS CONTAINING AROMATIC HYDROCARBONS TO PRODUCE VOLATILE AROMATIC SUBSTANCES

METHOD AND INSTALLATION FOR PRODUCING INTERMEDIATE PRODUCTS CONTAINING AROMATIC HYDROCARBONS TO PRODUCE VOLATILE AROMATIC SUBSTANCES

机译:生产包含芳烃的中间产物以生产挥发性芳烃的方法和装置

摘要

FIELD: coal-chemical industry. SUBSTANCE: invention relates to producing intermediate product to produce benzene from crude coal benzene where the latter is vaporized in stage 1 in evaporation column 2 to produce evaporation residue, while vaporized benzene reacts with hydrogen in pressure purification stage 3 connected with benzene evaporation stage 1 to form above-named intermediate product. According to invention, evaporation residue from evaporation stage 1 is tapped off and, in distillation stage 4, is separated into low- and high-boiling fractions, the latter being withdrawn as sump stream. Amount of tapped off evaporation residue is determined by concentration of polymerizing substances in crude coal benzene within the range 6 to 40% based on weight of raw material stream. Low-boiling fraction of evaporation residue withdrawn from distillation stage 4 is further condensed and fed into top part of evaporation column 2 as reflux stream. In distillation stage 4, double parameter gas pressure/temperature is established to indicate that sump stream is virtually free of aromatic hydrocarbons with less than 9 C atoms (excepting styrene). Corresponding installation is also provided. EFFECT: enhanced efficiency of process. 10 cl, 1 dwg
机译:领域:煤化工。本发明涉及生产中间产物以从粗煤苯生产苯,其中粗煤苯在阶段1中在蒸发塔2中蒸发以产生蒸发残余物,而蒸发的苯在与苯蒸发阶段1相连的压力纯化阶段3中与氢气反应,从而制得苯。形成上述中间产品。根据本发明,将来自蒸发阶段1的蒸发残余物排出,并且在蒸馏阶段4中,将其分为低沸点馏分和高沸点馏分,后者作为集料流取出。排出的蒸发残余物的量由粗煤苯中聚合物质的浓度(基于原料流的重量)在6%至40%的范围内确定。从蒸馏阶段4抽出的蒸发残留物的低沸点馏分进一步冷凝,并作为回流物流进料到蒸发塔2的顶部。在蒸馏阶段4中,建立了双参数气压/温度,以指示集液流实际上不含碳原子数少于9的芳族烃(苯乙烯除外)。还提供了相应的安装。效果:提高了流程效率。 10厘升,1载重吨

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