METHOD OF DEHYDRATING LITHIUM PERCHLORATE TRIHYDRATE

摘要

FIELD: inorganic synthesis. SUBSTANCE: lithium perchlorate trihydrate, finding use as electrolyte salt when manufacturing chemical power sources, is dehydrated to moisture content below 0.05% in apparatus with air medium at 50-60 C. Temperature is raised to the value of critical point of water (374 ± 5 C) and maintained for at least 5 min, after which lithium perchlorate melt obtained is transferred into box with dried air. Hardened material is abraded. EFFECT: optimized process parameters. 1 dwg