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Reaction injection molding of silicon nitride ceramics, with a crystalline grain boundary phases
Reaction injection molding of silicon nitride ceramics, with a crystalline grain boundary phases
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机译:具有晶界相的氮化硅陶瓷的反应注射成型
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摘要
A sintered, Si.sub.3 N.sub.4 -containing ceramic article is prepared by a reaction injection molding process comprising (1) injecting into a heated mold a fluid, nondilatant mixture of (a) at least 40% by volume of a powder mixture of (i) Si.sub.3 N.sub.4, (ii) a silicate glass- forming sintering aid and (iii) a high metal content silicide, and (b) a curable Si.sub.3 N.sub.4 precursor binder, to cure the binder and produce a hardened molded article, and (2) heating the molded article under a suitable atmosphere to convert the cured binder to a Si.sub.3 N.sub.4 - containing ceramic. The molded article is then sintered under a vacuum to crystallize the silicate glass phase by deoxygenation.
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机译:烧结的含Si 3 N 4的陶瓷制品是通过反应注射成型工艺制备的,该工艺包括(1)将(a)至少40%(体积)的液态非膨胀混合物注入加热的模具中。 (i)Si.sub.3 N.sub.4,(ii)形成硅酸盐玻璃的烧结助剂和(iii)高金属含量硅化物和(b)可固化Si.sub.N的粉末混合物SUB 4的前体粘合剂,以固化粘合剂并生产硬化的模制品,以及(2)在适当的气氛下加热模制品,以将固化的粘合剂转化为含Si 3 N 4的陶瓷。然后在真空下烧结模制品,以通过脱氧使硅酸盐玻璃相结晶。
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